Abstract: (5672 Views)
Iron oxide nanoparticles has attracted extensively due to their supermagnetic properties, preferred in biomedicine because of their biocompatibility and potential nontoxicity to human beings. Synthesis of iron nanoparticles (FeNPs) was prepared with the help of ferric chloride and ferrous sulphate by using the coprecipitation method. The variation and combination of ferric and ferrous concentrations affect the physical and magnetic properties of iron oxide nanoparticles. The effect of 0.1 M ferric and ferrous concentration on iron oxide nanoparticles studied separately and in combination. The obtained nanoparticles were characterized by Particle size, zeta potential, Ultraviolet (UV-visible), Fourier Transform Infrared Spectroscopy (FTIR), X-ray diffraction (XRD), Scanning electron microscope (SEM), Thermal gravimetric analysis (TGA), and Vibrating-sample magnetometer (VSM) techniques. Particle size was below 200nm and zeta potential was within the limit for all the batches. UV visible spectra at 224 nm, and FTIR exhibit two peaks at 510 and 594 cm-1, indicating iron oxide NPs and XRD confirmed the crystalline nature of Fe. SEM showed a spherical shape for all batches. The use of a combination of ferric and ferrous is more effective than its individual use. TGA and VSM studies confirmed its magnetic properties.
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Highlights:
- Synthesis Method: Adoption of the coprecipitation method using ferric chloride and ferrous sulphate, showcasing a widely used and scalable Technique.
- Concentration Influence: Investigation of the impact of varying concentrations of ferric and ferrous ions on the physical and magnetic properties of IONPs.
- Combination Synergy: Recognition of the enhanced effectiveness when using a combination of ferric chloride and ferrous sulphate, leading to uniform size, shape, crystalline nature, stability, and magnietization.
Type of Study:
Research Paper |
Subject:
Biomaterials