Volume 8, Number 2 (spring 2011 2011)                   IJMSE 2011, 8(2): 1-9 | Back to browse issues page


XML Print


Download citation:
BibTeX | RIS | EndNote | Medlars | ProCite | Reference Manager | RefWorks
Send citation to:

R. Taherzadeh Mousavian, S. Sharafi, M. H. Shariat. PREPARATION OF NANO-STRUCTURAL Al2O3-TiB2 IN-SITU COMPOSITE USING MECHANICALLY ACTIVATED COMBUSTION SYNTHESIS FOLLOWED BYINTENSIVE MILLING. IJMSE. 2011; 8 (2) :1-9
URL: http://ijmse.iust.ac.ir/article-1-335-en.html

Abstract:   (7212 Views)
Abstract: Nano-structural synthesized materials can be fabricated utilizing intensive milling after combustion synthesis. The Al2O3-TiB2 ceramic composite has been synthesized by aluminothermic reactions between Al, Ti (TiO2), and B (B2O3 or H3BO3). Boric acid (H3BO3) is less expensive than boron oxide, and after being dehydrated at 200°C, boron oxide will be obtained. In this study, Al, TiO2, and boric acid were used as the starting materials to fabricate an Al2O3-TiB2 ceramic composite. After mechanical activation and thermal explosion processes, intensive milling was performed for 5, 10, and 20h to assess the formation of a nano-structural composite. The X-ray phase analysis of the as-synthesized sample showed that considerable amounts of the remained reactants incorporated with the TiO phase were present in the XRD pattern. The results showed that the average crystallite size for alumina as a matrix were 150, 55 and 33 nm, after 5h, 10h, and 20h of intensive milling, respectively. The SEM microstructure of the as-milled samples indicated that increasing the milling duration after combustion synthesis causes a significant reduction in the particle size of the products, which leads to an increase in the homogeneity of particles size. A significant increase in the microhardness values of the composite powders was revealed after intensive milling process.
Full-Text [PDF 960 kb]   (1999 Downloads)    
Type of Study: Research paper |

Add your comments about this article : Your username or email:
Write the security code in the box

Send email to the article author


© 2016 All Rights Reserved | Iranian Journal of Materials Science and Engineering

Designed & Developed by : Yektaweb